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The Sythesis And Characterization Of Phthalocyanine/PAN Compound Nanomaterial

Posted on:2011-01-09Degree:MasterType:Thesis
Country:ChinaCandidate:J WangFull Text:PDF
GTID:2121360305989369Subject:Physical chemistry
Abstract/Summary:PDF Full Text Request
The solvethermal and electrospinning method to sythesize the Pc/PAN nano-fiber compound was tried in this paper. The PAN which was served as carrier combined with the 1,2-dicyanobenzene by sol-gel process, then the solution was processed into the precursor which was added into glycol together with Cd,Ni,Cu phthalocyanine compound in reactionkettle. The effects of the variations in concentration and reaction time on the morphology of Pc were studied. The products were characterized by scanning electron microscope (SEM), infrared spectra (IR), ultravidet sprctra (UV-vis).The results show that (1) The morphology and particle size of PC varied due to different metals Ni, Cd, Cu as ligands sin Pc/PAN. (2) The concentration influenced the morphology greatly, Cd-Pc on the fiber were cube and sphere respectively with different concentrations. (3) The time of this reaction also influencued the morphology, Cd-Pc on the fiher were cube,cotton and thorn respectively with different times.
Keywords/Search Tags:phthalocyanine nano-fiber, Synthesis, Characterization, Electrospinning solvethermal, morphology
PDF Full Text Request
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