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Fabrication and characterization of lead zirconate titanate nanorods and nanohexagons with applications in piezoelectric transducers

Posted on:2013-06-19Degree:M.SType:Thesis
University:University of Alberta (Canada)Candidate:Wan, QianFull Text:PDF
GTID:2451390008466028Subject:Engineering
Abstract/Summary:
All ultrasound devices/sensors use piezoelectric transducers to generate/receive ultrasound. These transducers are made of Pb (Zr 0.53Ti0.47) O3 (PZT) materials. In this article, we report a new way of fabricating PZT material with interesting nanorod and nanohexagon shapes. The PZT nanohexagons with typical diameters and bounding lengths within the nanometer range were synthesized by sintering a mixture of PZT nanocrystals, Tween 20 and sodium chloride, in which the PZT nanocrystals were made by a sol-gel method. The PZT nanorods were also synthesized by sintering a mixture of PZT nanocrystals, Triton and sodium chloride. After annealing at 800°C for three hours, PZT nanorods and PZT nanohexagons formed and exhibited a single-crystalline nanostructure, confirmed by high resolution transmission electronic microscopy (HRTEM). X-ray diffraction (XRD) and Raman Spectra studies demonstrated their crystal structures and composition, scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used to image their morphologies.
Keywords/Search Tags:PZT, Nanorods, Nanohexagons
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