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The Microstructures And Properties Of In-Situ Prepared Mg2Sip/Mg-Al Matrix Composites And Its' Extrusion Deformation

Posted on:2008-12-27Degree:MasterType:Thesis
Country:ChinaCandidate:S Z JiaFull Text:PDF
GTID:2121360212479629Subject:Materials Physics and Chemistry
Abstract/Summary:PDF Full Text Request
in-situ reaction. The effects of the traditional solidification,extrusion and reciprocating extrusion and different heat treatment on microstructures and properties of the composites were investigated. The microstructures and phase constitution of the composites which were prepared by different techniques were studied by optical microscope, scanning electronic microscope, X-ray diffraction and differential thermal analysis. The mechanical properties of the composites were measured by hardness and tensile tests, and the thermal expansibilities of all composites prepared by different techniques were also tested by thermal mechanical analysis. The conclusions are as follows:1. AS93, AS96 and AS99 magnesium matrix composites were prepared by adding Al-Si intermediate alloy into magnesium alloy melt. The microstructures of these composites series are composed ofα-Mg matrix, dendritic or polygonal Mg2Si phase andβ-Mg17Al12 phase.2. After solution treated composite ingots are extruded, complete recrystallization of AS93 matrix has happened; broken and refined Mg2Si phases are distributed strippedly along direction of extrusion. AS96 has only partial recrystallization; the extruded and broken Mg2Si are distributed strippedly in form of comparatively large block along direction of extrusion. Basal body of AS99 is extruded and elongated into strip tape, equiaxed crystals aren't discovered in the basal body; the extruded Mg2Si only are extruded and broken, but not separated.3. The uniform and refining microstructures which Mg2Si particles uniformly distribute inmaybe obtained through reciprocately extruding solutioned Mg2Si/Mg-Al matrix composites. As RE passes increase, Mg2Si phases are broken and refined gradually; the size of the basal body crystal grain also diminishes gradually. The size of the basal body crystal grain of RE-12P is less than 10μm, equiaxed Mg2Si particles which are less than 20μm distribute uniformly in the basal body. 4. RE can greatly improve mechanical properties of as-cast Mg2Si/Mg-Al matrixcomposites. As RE passes increase, room temperature and elevated temperature tensile properties, compressive property and hardness are improved greatly.
Keywords/Search Tags:Mg2Si phase, magnesium matrix composites, extrusion, reciprocating extrusion (RE)
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